Repeat the methanol draining procedure while making sure the gels stay submerged in liquid CO2. Repeat the CO2 draining/exchange a couple ... Posted by Ben Krasnow at 2:27 PM. Labels: aerogel, aerogel at home, aerogel production, supercritical, supercritical drying, tetramethoxysilane, tetramethyl orthosilicate, xerogel .... The glass window in my steel chamber came from McMaster (it is a high-pressure, plain "sight glass"). My plastic chamber is built from 1.25"& ...
make orthosilicate glass
Editor`s Note: This is an adaptation of the silica aerogel procedure from the Lawrence Berkeley National Laboratory site about aerogels, which for a long time was the only procedure for making aerogels publicly available. That procedure, we`re sorry to say, does not work. Maybe ... Materials. Tetraethoxysilane (tetraethyl orthosilicate), Si(OC2H5)4; Absolute (200-proof) ethanol; Deionized water; Ammonium hydroxide, 28-30 wt % in water; Ammonium fluoride, NH4F. Optional. Acetone& ...
Mesoporous bioactive glasses (MBGs) doped with Ti/Ag were synthesized. The structural, morphological, and textural properties of all samples were investigated by small-angle X-ray diffraction (XRD), scanning electron microscopy (SEM),& ...
As a result of its high specific surface area, large pore volume, and mesoporous structure, MBG exhibits the enhanced bone-forming bioactivity, degradation and drug delivery properties, compared to the conventional bioactive glass (BG) [3–10]. .... As an example, to prepare magnetic Fe-MBG/C composite scaffolds containing 10% Fe (10Fe-MBG/C), typically 4.0 g of P123 (Mw = 5800, Aldrich), 6.7 g of tetraethyl orthosilicate (TEOS, 98%, Acros), 0.47 g of calcium nitrate (Ca (NO 3)& ...
Repeat the methanol draining procedure while making sure the gels stay submerged in liquid CO2. Repeat the CO2 draining/exchange a couple ... Posted by Ben Krasnow at 2:27 PM. Labels: aerogel, aerogel at home, aerogel production, supercritical, supercritical drying, tetramethoxysilane, tetramethyl orthosilicate, xerogel .... The glass window in my steel chamber came from McMaster (it is a high-pressure, plain "sight glass"). My plastic chamber is built from 1.25"& ...
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- Sep 01 Sun 2013 03:10
Make Orthosilicate Glass
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Make Orthosilicate Glass
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